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dc.contributor.authorFiamegos, Y. C.en
dc.contributor.authorPilidis, G. A.en
dc.contributor.authorVarvounis, G.en
dc.date.accessioned2015-11-24T16:49:12Z-
dc.date.available2015-11-24T16:49:12Z-
dc.identifier.issn0022-152X-
dc.identifier.urihttps://olympias.lib.uoi.gr/jspui/handle/123456789/9445-
dc.rightsDefault Licence-
dc.subjectagentsen
dc.titleSynthesis of 1-methyl-, 4-nitro-, 4-amino- and 4-iodo-1,2-dihydro-3H-pyrazol-3-onesen
heal.typejournalArticle-
heal.type.enJournal articleen
heal.type.elΆρθρο Περιοδικούel
heal.identifier.secondary<Go to ISI>://000171704700009-
heal.identifier.secondaryhttp://onlinelibrary.wiley.com/store/10.1002/jhet.5570380509/asset/5570380509_ftp.pdf?v=1&t=hmrggkvh&s=d55975fee7cf5a1cb344b53bdf95c7345442a0b3-
heal.languageen-
heal.accesscampus-
heal.recordProviderΠανεπιστήμιο Ιωαννίνων. Σχολή Θετικών Επιστημών. Τμήμα Χημείαςel
heal.publicationDate2001-
heal.abstract4-Aminopyrazole-3-ones 4b, e, f were prepared from pyrazole-3-ones 1b-d in a four-step reaction sequence. Reaction of the latter with methyl p-toluenesulfonate gave 1-methylpyrazol-3-ones 2b-d. Compounds 2b-d were treated with aqueous nitric acid to give 4-nitropyrazol-3-ones 3b-d. Reduction of compounds 3b-d by catalytic hydrogenation with Pd-C afforded the 4-amino compounds 4b, e, C Using similar reaction conditions, nitropyrazole-3-ones derivatives 2c, d were reduced into aminopyrazole-3-ones 5e, f. 4-lodopyrazole-3-ones 7a, 7c and 8 were prepared from the corresponding pyrazol-3-ones 2a, 2c and 6 and iodine monochloride or sodium azide and iodine monochloride.en
heal.publisherWiley-Blackwellen
heal.journalNameJournal of Heterocyclic Chemistryen
heal.journalTypepeer reviewed-
heal.fullTextAvailabilityTRUE-
Appears in Collections:Άρθρα σε επιστημονικά περιοδικά ( Ανοικτά). ΧΗΜ

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