Please use this identifier to cite or link to this item: https://olympias.lib.uoi.gr/jspui/handle/123456789/17051
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dc.contributor.authorVlachos, Dimitrios,en
dc.contributor.authorCraven, Alan J.,en
dc.contributor.authorMcComb, David W.,en
dc.date.accessioned2015-11-24T18:35:08Z-
dc.date.available2015-11-24T18:35:08Z-
dc.identifier.issn0909-0495-
dc.identifier.urihttps://olympias.lib.uoi.gr/jspui/handle/123456789/17051-
dc.rightsDefault Licence-
dc.subjectX-ray absorption near-edge structureen
dc.subjectelectron energy-loss near-edge structureen
dc.subjectchargingen
dc.subjectcorrection for chargingen
dc.subjecttotal electron yielden
dc.titleSpecimen charging in X-ray absorption spectroscopy: correction of total electron yield data from stabilized zirconia in the energy range 250-915 eVen
heal.typejournalArticle-
heal.type.enJournal articleen
heal.type.elΆρθρο Περιοδικούel
heal.identifier.primarydoi:10.1107/S0909049504030146-
heal.identifier.secondaryhttp://dx.doi.org/10.1107/S0909049504030146-
heal.accesscampus-
heal.recordProviderΠανεπιστήμιο Ιωαννίνων. Σχολή Επιστημών και Τεχνολογιών. Τμήμα Βιολογικών Εφαρμογών και Τεχνολογιώνel
heal.publicationDate2005-
heal.abstractThe effects of specimen charging on X-ray absorption spectroscopy using total electron yield have been investigated using powder samples of zirconia stabilized by a range of oxides. The stabilized zirconia powder was mixed with graphite to minimize the charging but significant modifications of the intensities of features in the X-ray absorption near-edge fine structure (XANES) still occurred. The time dependence of the charging was measured experimentally using a time scan, and an algorithm was developed to use this measured time dependence to correct the effects of the charging. The algorithm assumes that the system approaches the equilibrium state by an exponential decay. The corrected XANES show improved agreement with the electron energy-loss near-edge fine structure obtained from the same samples.en
heal.journalNameJ Synchrotron Radiaten
heal.journalTypepeer reviewed-
heal.fullTextAvailabilityTRUE-
Appears in Collections:Άρθρα σε επιστημονικά περιοδικά ( Ανοικτά) - ΦΥΣ



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