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dc.contributor.authorTsiafoulis, C. G.en
dc.contributor.authorNanos, C. G.en
dc.date.accessioned2015-11-24T16:55:32Z-
dc.date.available2015-11-24T16:55:32Z-
dc.identifier.issn0013-4686-
dc.identifier.urihttps://olympias.lib.uoi.gr/jspui/handle/123456789/10322-
dc.rightsDefault Licence-
dc.subjecthoneyen
dc.subjectorganophosphorus insecticidesen
dc.subjectstandard addition methoden
dc.subjectpesticidesen
dc.subjectquantitation protocolen
dc.subjectchromatography-mass spectrometryen
dc.subjectsolid-phase extractionen
dc.subjectgas-chromatographyen
dc.subjectelectron-captureen
dc.subjectorganophosphorus pesticidesen
dc.subjectpolarographic-determinationen
dc.subjectinjection-analysisen
dc.subjectmicroelectrodesen
dc.subjectinsecticidesen
dc.subjectresiduesen
dc.titleDetermination of azinphos-methyl and parathion-methyl in honey by stripping voltammetryen
heal.typejournalArticle-
heal.type.enJournal articleen
heal.type.elΆρθρο Περιοδικούel
heal.identifier.primaryDOI 10.1016/j.electacta.2010.09.009-
heal.identifier.secondary<Go to ISI>://000285177800077-
heal.identifier.secondaryhttp://ac.els-cdn.com/S0013468610011680/1-s2.0-S0013468610011680-main.pdf?_tid=4f47f7b7111640b7996288c750cc2935&acdnat=1333035269_1b0c83180726ef8ece64e5c9b5c5aa14-
heal.languageen-
heal.accesscampus-
heal.recordProviderΠανεπιστήμιο Ιωαννίνων. Σχολή Θετικών Επιστημών. Τμήμα Χημείαςel
heal.publicationDate2010-
heal.abstractAn electrochemical method for the determination of azinphos-methyl and parathion-methyl in honey is presented. The determination is established by adsorptive stripping differential pulse voltammetry at hanging mercury working electrode. In contrast to the chromatographic methods for the determination of pesticide residues, the sample preparation of the proposed method is minimal; analytes were extracted from honey samples with a mixture of (acetone):(Britton-Robinson buffer) and then were analyzed without any additional pretreatment. The response of the analytes either individually or as a mixture was studied for a series of deposition time and molar ratio. Two quantitation protocols were compared, using either the external calibration or the standard addition method. Accuracy was tested with spiked honey samples obtaining good recovery values. The limit of detection for the honey sample (for deposition time of 10 s) was calculated 51.71 mu g kg(-1) for MeP and 65.87 mu g kg(-1) for AzMet. (C) 2010 Elsevier Ltd. All rights reserved.en
heal.publisherElsevieren
heal.journalNameElectrochimica Actaen
heal.journalTypepeer reviewed-
heal.fullTextAvailabilityTRUE-
Appears in Collections:Άρθρα σε επιστημονικά περιοδικά ( Ανοικτά). ΧΗΜ

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