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DC Field | Value | Language |
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dc.contributor.author | Tsogas, G. Z. | en |
dc.contributor.author | Stergiou, D. V. | en |
dc.contributor.author | Vlessidis, A. G. | en |
dc.contributor.author | Evmiridis, N. P. | en |
dc.date.accessioned | 2015-11-24T16:56:01Z | - |
dc.date.available | 2015-11-24T16:56:01Z | - |
dc.identifier.issn | 0003-2670 | - |
dc.identifier.uri | https://olympias.lib.uoi.gr/jspui/handle/123456789/10380 | - |
dc.rights | Default Licence | - |
dc.subject | propranolol determination | en |
dc.subject | chemiluminescence detection | en |
dc.subject | flow injection analysis | en |
dc.subject | pyrogallol | en |
dc.subject | periodate | en |
dc.subject | pharmaceutical-preparations | en |
dc.subject | capillary electrophoresis | en |
dc.subject | liquid-chromatography | en |
dc.subject | mass-spectrometry | en |
dc.subject | pyrogallol | en |
dc.subject | oxidation | en |
dc.subject | periodate | en |
dc.subject | hcl | en |
dc.title | Development of a sensitive flow injection-chemiluminescence detection method for the indirect determination of propranolol | en |
heal.type | journalArticle | - |
heal.type.en | Journal article | en |
heal.type.el | Άρθρο Περιοδικού | el |
heal.identifier.primary | DOI 10.1016/j.aca.2004.11.074 | - |
heal.identifier.secondary | <Go to ISI>://000229648500019 | - |
heal.identifier.secondary | http://ac.els-cdn.com/S0003267004016290/1-s2.0-S0003267004016290-main.pdf?_tid=cde0264c-356a-11e3-9e6d-00000aacb35f&acdnat=1381822038_e7e129de2c68c14f6d7b142c4307a10a | - |
heal.language | en | - |
heal.access | campus | - |
heal.recordProvider | Πανεπιστήμιο Ιωαννίνων. Σχολή Θετικών Επιστημών. Τμήμα Χημείας | el |
heal.publicationDate | 2005 | - |
heal.abstract | A highly sensitive flow injection-chemiluminescence detection (FI-CL) method based on pyrogallol (Pg) chemiluminescentreagent (CL-reagent) oxidized by periodate for the determination of propranolol is presented. The presented method is an indirect CL detection method based on the CL emission generated during the oxidation of Pg with the excess of periodate that remains after oxidation of propranolol within the time period of 10 min. The obtained propranolol calibration curve is linear up to 1.0 mg(-1) with a sensitivity of -0.95 V mg(-1). At higher than 1.0 mg l(-1) propranolol concentrations the propranolol calibration curve is still linear up to 20.0 mg l(-1) with a sensitivity of -0.05 V mg(-1) 1. The detection limit is restricted from the noise level and at S/N = 3 was found to be 37.4 mu g l(-1) (3.74 ng) with R.S.D.% = 0.34 for seven replicate measurements. (c) 2004 Elsevier B.V. All rights reserved. | en |
heal.publisher | Elsevier Masson | en |
heal.journalName | Analytica Chimica Acta | en |
heal.journalType | peer reviewed | - |
heal.fullTextAvailability | TRUE | - |
Appears in Collections: | Άρθρα σε επιστημονικά περιοδικά ( Ανοικτά). ΧΗΜ |
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Tsogas-2005-Development of a sen.pdf | 159.56 kB | Adobe PDF | View/Open Request a copy |
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